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The thermal decomposition of ferrous oxalate dihydrate 1603 pure anhydrous material. Watervapourdoes not appear to catalyse the decomposition of the anhydrous material as may have been suggested by the extremely rapid rate at which the dihydrate decomposes in dry oxygen.
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of oxalate ion. Additional data will be provided to calculate the mass percent of iron, water and potassium so the empirical formula can be determined. !! The mass percent oxalate ion in the salt will be determined by titration with a standardized ! KMnO 4 solution according to the unbalanced reaction below: !! (1) MnO 4 (aq) + C 2O 4
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The action of heat on ferrous oxalate dihydrate results in dehydration, followed almost immediately by decomposition. The anhydrous salt can, however, be isolated, and X ray powder diffraction data, not previously available in detail, are given for the anhydrous phase.
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